FACTORS AFFECTING THE ASSAY OF HYALURONIDASE

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Factors affecting the assay of hyaluronidase.

A number of different types of assay methods have been developed for the determination of hyaluronidase activity in vitro. These include the mucin clot test (1, 2), the viscosimetric assay (3-12), the turbidimetric assay (7, 13-17), and the reductimetric assay (18). Of these, the turbidimetric and viscosimetric assays have been used most widely. In the work reported here a study has been made o...

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Hyaluronidase: correlation between biological assay and other methods of assay.

Different workers have at various times sought to correlate the in vivo and in vitro activities of hyaluronidase preparations. Chain & Duthie (1940), drawing attention to the association between diffusion in the tissues and the mucolytic activity of testicular extracts, pointed out that the viscosityreducing and diffusing activities of various enzyme preparations were in good agreement. McClean...

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Quantitative micro-scale complement-fixation and semi-quantitative gel immunodiffusion assays for myoglobin have been evaluated experimentally and used to measure myoglobin in the sera of more than 1500 patients. We report certain problems, observations, and methodological improvements. Serum caused enhancement of precipitin lines in the immunodiffusion assay. In the complement-fixation assay,...

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Factors affecting a cyanogen bromide-based assay of thiamin.

We analyzed extensively a modified thiochrome method for thiamin analysis. Acid phosphatase (EC 3.1.3.2) from potato was superior to either alpha-amylase or acid phosphatase from wheat germ as a dephosphorylating agent. Timing of cyanogen bromide exposure was important, but the assay had good precision and accuracy. The standard curve was linear from 10 to 3000 nmol/L. The within-run and betwee...

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A turbidimetric method for the assay of hyaluronidase.

A variety of methods have been devised for the assay of the enzyme hyaluronidase. These may be divided into four types: (a) measurement of the “spreading effect” in the skin of rabbits and guinea pigs (1, 2), (b) reduction of viscosity (3,4), (c) prevention of mucin clot formation (5), and (d) chemical measurement of total reducing substances, N-acetylglucosamine, or glucuronic acid liberated o...

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ژورنال

عنوان ژورنال: Journal of Biological Chemistry

سال: 1951

ISSN: 0021-9258

DOI: 10.1016/s0021-9258(18)55942-1